排序方式: 共有6条查询结果,搜索用时 328 毫秒
1
1.
2.
GPC-GC/MS法分析血中20种安眠镇静药物 总被引:1,自引:0,他引:1
目的研究建立液液提取-在线GPC-GC/MS同时分析血中巴比妥类、吩噻嗪类、苯并二氮杂卓类、三环类和其他安眠精神类药物的方法。方法血样加入内标SKF525A,加β-葡萄糖酸苷酶水解后用乙腈沉淀蛋白浸取药物,加无水硫酸镁脱水,提取液浓缩至干后用GPC流动相定容,在线GPC净化,大体积进样,GC-MS分析。结果选择总离子监测模式,血中20种安眠镇静药物提取率在80.2%~99.3%之间,检出限小于21.6ng/mL;在0.1~10μg/mL浓度范围内工作曲线的线性关系良好。结论方法可用于安眠镇静类药物误服中毒者和刑事案件中毒者血样的分析。 相似文献
3.
4.
5.
Abstract The aims of this study were to assess the impact of public conceptions about the nature and coercive powers of hypnosis, and information regarding different approaches to hypnosis, on the plea of automatism through hypnosis in a criminal trial. Subjects were assigned to three groups. Two were presented with criminal cases in which automatism through hypnosis was implicated, as well as duress; one of these groups received information about different approaches to hypnosis. The third received the same cases, but with duress alone. Results showed that, when automatism through hypnosis was implicated as well as duress, the defendant offering the plea was judged less responsible, however, he was not judged less guilty than when duress alone was the defence. Also, subjects presented with the plea of automatism tended to be more sceptical about the idea than those not presented with this plea. The provision of information on different approaches to hypnosis was largely ineffective in altering beliefs and judgments. Judgments of guilt and responsibility were, however, strongly influenced by beliefs about automatism through hypnosis. 相似文献
6.
1